ASTM D6144 - 17 - Standard Test Method for Analysis of AMS (α-Methylstyrene) by Capillary Gas Chromatography

ASTM D6144 - 17

Standard Test Method for Analysis of AMS (α-Methylstyrene) by Capillary Gas Chromatography

Status : Current   Published : June 2017

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1.1 This test method covers the determination of the purity of AMS (α-methylstyrene) by gas chromatography. Calibration of the gas chromatography system is done by the external standard calibration technique.

1.2 This test method has been found applicable to the measurement of impurities such as cumene, 3-methyl-2-cyclopentene-1-one, n-propylbenzene, tert-butylbenzene, sec-butylbenzene, cis-2-phenyl-2-butene, acetophenone, 1-phenyl-1-butene, 2-phenyl-2-propanol, trans-2-phenyl-2-butene, m-cymene, p-cymene, and phenol, which are common to the manufacturing process of AMS. The method has also been found applicable for the determination of para-tertiary-butylcatechol typically added as a stabilizer to AMS. The impurities in AMS can be analyzed over a range of 5 to 800 mg/kg by this method. (See Table 1.) The limit of quantitation for these these impurities averages 4 mg/kg, while the limit of detection averages 1.2 mg/kg. (See Table 1.)

TABLE 1 Summary of Precision Data (mg/kg)

[This table has been removed.]

1.3 In determining the conformance of the test results using this method to applicable specifications, results shall be rounded off in accordance with the rounding-off method of Practice E29.

1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.5  This standard does not purport to address all the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see Section 8.

1.6  This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.




Standard NumberASTM D6144 - 17
TitleStandard Test Method for Analysis of AMS (α-Methylstyrene) by Capillary Gas Chromatography
StatusCurrent
Publication Date01 June 2017
Normative References(Required to achieve compliance to this standard)No other standards are normatively referenced
Informative References(Provided for Information)No other standards are informatively referenced
Descriptors Chemical separation Concentration Hydrous manganese oxide Manganese oxide Pre-concentration
ICS71.040.50
PublisherASTM
FormatA4
DeliveryYes
Pages5
File Size146 KB
Price£40.00


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