BS EN 17212:2019 - Animal Feeding stuffs. Methods of sampling and analysis. Determination of melamine and cyanuric acid content by liquid chromatographic method with mass spectrometric detection (LC-MS/MS)

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BS EN 17212:2019

Animal Feeding stuffs. Methods of sampling and analysis. Determination of melamine and cyanuric acid content by liquid chromatographic method with mass spectrometric detection (LC-MS/MS)

Status : Current   Published : September 2019

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This document specifies a high-performance liquid chromatographic (HPLC) mass spectrometric (MS) method for screening and quantification of melamine and cyanuric acid in the concentration range between 1 mg/kg and 100 mg/kg feed. The method is validated in an international collaborative trial for melamine in complete feed, complementary feed, feed material, milk replacer and pet food including canned pet food in the range between 1 mg/kg and 80 mg/kg with particular regard to the maximum level of 2,5 mg/kg as established by the European Commission. Laboratory experiences have shown that the method is also applicable for cyanuric acid in the same concentration range in complete feed (n = 7), complementary feed (n = 6), feed material (n = 7, resp. 9), milk replacer (n = 7) and pet food (n = 7) including canned pet food. Since the LC-MS/MS sensitivity for cyanuric acid is lower than for melamine, it has to be ensured that the LC-MS/MS system is in excellent working order. The method is applicable to feeding stuffs but not tested for pre-mixtures and feed additives. Quantification of concentrations above 100 mg/kg is possible, but the method has to be validated by the operator.




Standard NumberBS EN 17212:2019
TitleAnimal Feeding stuffs. Methods of sampling and analysis. Determination of melamine and cyanuric acid content by liquid chromatographic method with mass spectrometric detection (LC-MS/MS)
StatusCurrent
Publication Date12 September 2019
Cross ReferencesISO 3534-2:2006, EN ISO 6498:2012, EN ISO/IEC 17043:2010, ISO/IEC Guide 99:2007, ISO 24276:2006, ISO 16577:2016, EN ISO 6497, ISO 5725-2:2019, BS ISO 5725-2:2019, ISO 11843-2, ISO 5725-1
International RelationshipsEN 17212:2019
Draft Superseded By17/30337117 DC
DescriptorsMass, Liquid chromatography, Determination of content, Cyanuric acid, Melamine, Analysis, Feed (animal)
ICS65.120
Title in FrenchAliments des animaux. Méthodes d'échantillonnage et d'analyse. Détermination des teneurs en mélanine et en acide cyanurique par chromatographie liquide couplée à la spectrométrie de masse (LC-MS/MS)
Title in GermanFuttermittel. Probenahme- und Untersuchungsverfahren. Bestimmung des Gehaltes von Melamin und Cyanursäure mittels flüssigkeitschromatographischem Verfahren mit massenspektrometrischem Nachweis (LC-MS/MS)
CommitteeAW/10
ISBN978 0 580 93223 6
PublisherBSI
FormatA4
DeliveryYes
Pages40
File Size1.59 MB
Price£214.00


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