ASTM D7151 - 15 - Standard Test Method for Determination of Elements in Insulating Oils by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES)

ASTM D7151 - 15

Standard Test Method for Determination of Elements in Insulating Oils by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES)

Status : Current   Published : January 2015

Format
PDF

Format
HARDCOPY



1.1 This test method describes the determination of metals and contaminants in insulating oils by inductively coupled plasma atomic emission spectrometry (ICP-AES). The specific elements are listed in Table 1. This test method is similar to Test Method D5185, but differs in methodology, which results in the greater sensitivity required for insulating oil applications.

(A)  These wavelengths are only suggested and do not represent all possible choices.

1.2 This test method uses oil-soluble metals for calibration and does not purport to quantitatively determine insoluble particulates. Analytical results are particle size dependent, and low results are obtained for particles larger than several micrometers. 2

1.3 This test method determines the dissolved metals (which can originate from overheating or arcing, or both) and a portion of the particulate metals (which generally originate from a wear mechanism). While this ICP method detects nearly all particles less than several micrometers, the response of larger particles decreases with increasing particle size because larger particles are less likely to make it through the nebulizer and into the sample excitation zone.

1.4 This test method includes an option for filtering the oil sample for those users who wish to separately determine dissolved metals and particulate metals (and hence, total metals).

1.5 Elements present at concentrations above the upper limit of the calibration curves can be determined with additional, appropriate dilutions and with no degradation of precision.

1.6 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.7  This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and to determine the applicability of regulatory limitations prior to use.




Standard NumberASTM D7151 - 15
TitleStandard Test Method for Determination of Elements in Insulating Oils by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES)
StatusCurrent
Publication Date05 January 2015
Normative References(Required to achieve compliance to this standard)No other standards are normatively referenced
Informative References(Provided for Information)No other standards are informatively referenced
Descriptors Aluminum, Cadmium, Copper, Emission-spectrometry, ICP, Inductively coupled plasma atomic emission spectrometry, Insulating liquid, Iron, Lead, Silicon, Silver, Sodium, Tin, Transformer oil, Tungsten, Wear metals, Zinc
ICS29.040.10
PublisherASTM
FormatA4
DeliveryYes
Pages8
File Size96 KB
Price£40.00


 Your basket
Your basket is empty

Multi-user access to over 3,500 medical device standards, regulations, expert commentaries and other documents


BSOL

The faster, easier way to work with standards


Develop a PAS

Develop a fast-track standardization document in 9-12 months


Tracked Changes

Understand the changes made to a standard with our new Tracked Changes version