BS EN 16924:2017 - Foodstuffs. Determination of zearalenone in edible vegetable oils by LC-FLD or LC-MS/MS

BS EN 16924:2017

Foodstuffs. Determination of zearalenone in edible vegetable oils by LC-FLD or LC-MS/MS

Status : Current   Published : June 2017

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This European Standard describes a procedure for the determination of the zearalenone content in edible vegetable oils specifically maize germ oil by either of the following techniques: High performance liquid chromatography with fluorescence detection (LC-FLD) or high performance liquid chromatography with tandem mass spectrometry (LC-MS/MS) after basic extraction of the diluted oil. The method has been validated for zearalenone in naturally contaminated maize germ oil at levels of 61,2 µg/kg to 515 µg/kg [5]. Laboratory experiences [6] have shown that this method is also applicable to other vegetable oils such as wheat germ oil (n = 4), sunflower oil (n = 5), pumpkin seed oil (n = 1), soybean oil (n = 5), hemp seed oil (n = 5), rape seed oil (n = 11), and mixed oils including maize germ oil (n = 3). However occasionally, samples can result in interferences in the FLD-chromatograms. In this case, the detection with MS/MS is recommended.




Standard NumberBS EN 16924:2017
TitleFoodstuffs. Determination of zearalenone in edible vegetable oils by LC-FLD or LC-MS/MS
StatusCurrent
Publication Date21 June 2017
Normative References(Required to achieve compliance to this standard)EN ISO 3696, ISO 3696:1987, BS EN ISO 3696:1995
Informative References(Provided for Information)ISO/IEC 17025:2005, ISO 5725:1986, ISO 5725-2:1994, ISO 5725-6:1994, EN ISO/IEC 17025:2005, ISO 5725-4:1994, ISO 5725-5:1998, ISO 5725-3:1994, ISO 5725-1:1994
International RelationshipsEN 16924:2017
Draft Superseded By15/30324942 DC
DescriptorsVegetable oils, Oilseeds, Wood oil, Tung oil, Sunflower seed oil, Soya bean oil, Sesame oil, Safflower seed oil, Rape seed oil, Perilla oil, Cottonseed oil, Coconut oil, Castor oil, Camphorated oil, Plant extracts, Oils
ICS67.200.10
Title in FrenchProduits alimentaires. Dosage de la zéaralénone dans les huiles végétales alimentaires par CL-FLD ou CLSM/SM
Title in GermanLebensmittel. Bestimmung von Zearalenon in pflanzlichen Speiseölen mit LC-FLD oder LC-MS/MS
CommitteeAW/275
ISBN978 0 580 90470 7
PublisherBSI
FormatA4
DeliveryYes
Pages34
File Size0.998 MB
Price£214.00


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