BS EN 16691:2015 - Water quality. Determination of selected polycyclic aromatic hydrocarbons (PAH) in whole water samples. Method using solid phase extraction (SPE) with SPE-disks combined with gas chromatography mass spectrometry (GC-MS)

BS EN 16691:2015

Water quality. Determination of selected polycyclic aromatic hydrocarbons (PAH) in whole water samples. Method using solid phase extraction (SPE) with SPE-disks combined with gas chromatography mass spectrometry (GC-MS)

Status : Current, Under review   Published : September 2015

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This European Standard specifies a method for the determination of 7 polycyclic aromatic hydrocarbons (PAH) in whole water samples listed in Table 1. The method uses solid-phase disk extraction with SPE-disks followed by gas chromatography-mass spectrometry (GC-MS). It is applicable to the analysis of PAHs in surface water containing suspended particulate matter (SPM) up to 500 mg/l (whole water samples), drinking water and groundwater.

The lower and upper limit of the working range depends on the matrix, on the specific compound to be analyzed and on the sensitivity of the mass spectrometric detection unit. The limit of quantification (LOQ) determined in the validation is given in Table 1. The upper limit of the working range is approximately 2 000 ng/l.

This method is, with some modifications suitable for the analysis of waste water. This method is applicable to other PAH 1) , provided the method is validated for each PAH.

Table 1
Polycyclic aromatic hydrocarbons (PAH) determined by this method

[This table has been removed.]

a

EC Number: European inventory of existing commercial substances (EINECS) or European list of notified chemical substances (ELINCS).

b

CAS-RN: Chemical Abstracts Service Registry Number.

c

For the determination of the LOQ the procedure given in NEN 7777+C1:2012[12] was used.




Standard NumberBS EN 16691:2015
TitleWater quality. Determination of selected polycyclic aromatic hydrocarbons (PAH) in whole water samples. Method using solid phase extraction (SPE) with SPE-disks combined with gas chromatography mass spectrometry (GC-MS)
StatusCurrent, Under review
Publication Date30 September 2015
Normative References(Required to achieve compliance to this standard)ISO 5667-3, ISO 1042, EN ISO 3696, EN ISO 5667-1, ISO 3696, EN ISO 1042, ISO 5667-1, EN ISO 5667-3
Informative References(Provided for Information)ISO 7981-2, 2000/60/EC, ISO 28540, EN ISO 22892, NEN 7777+C1:2012, ISO 17993, ISO 7981-1, ISO/TS 13530, ISO 22892, EN ISO 17993, ISO/TS 28581, 2008/105/EC, SANCO/12571/2013, 2013/39/EU, ISO 8466-1, EN 15527, 2009/90/EC, ISO 5725-2:2019, ISO 6107-2, BS ISO 5725-2:2019
International RelationshipsEN 16691:2015
Draft Superseded By13/30290864 DC
DescriptorsWater, Fluorimetry, Extraction methods of analysis, Chromatography, Chemical analysis and testing, Potable water, Aromatic hydrocarbons, Polynuclear aromatic hydrocarbons, Quality, Thin-layer chromatography, Water testing, Determination of content
ICS13.060.50
Title in FrenchQualité de l'eau. Dosage des hydrocarbures aromatiques polycycliques (HAP) sélectionnés dans des échantillons d'eau totale. Méthode par extraction en phase solide (SPE) avec disques SPE, avec couplage chromatographie en phase gazeuse-spectrométrie de masse (CG-SM)
Title in GermanWasserbeschaffenheit. Bestimmung von ausgewählten polycyclischen aromatischen Kohlenwasserstoffen (PAK) in Gesamtwasserproben. Verfahren mittels Festphasenextraktion (SPE) mit SPE-Disks in Verbindung mit Gaschromatographie Massenspektrometrie (GC-MS)
CommitteeEH/3/2
ISBN978 0 580 84469 0
PublisherBSI
FormatA4
DeliveryYes
Pages36
File Size1.188 MB
Price£218.00


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