BS EN 16618:2015 - Food analysis. Determination of acrylamide in food by liquid chromatography tandem mass spectrometry (LC-ESI-MS/MS)

BS EN 16618:2015

Food analysis. Determination of acrylamide in food by liquid chromatography tandem mass spectrometry (LC-ESI-MS/MS)

Status : Current   Published : April 2015

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This European Standard specifies a method for the determination of acrylamide in bakery ware such as bread, toasted bread, crisp bread, butter cookies, and biscuits, as well as potato products such as potato chips, potato crisps, and potato pan cake and roasted coffee, by liquid chromatography in combination with electrospray ionization and tandem mass spectrometry (LC-ESI-MS/MS). This method has been validated in an interlaboratory study via the analysis of both naturally contaminated and spiked samples, ranging from 14,3 µg/kg to 9 083 µg/kg. It was developed at the Swedish National Food Administration and validated in a study organized by the Directorate General Joint Research Centre (DG JRC), Swedish National Food Administration and the Nordic Committee on Food Analysis (NMKL), see [1] and [2].

The limit of quantification (LOQ) depends on the type of instrument used and on the actual performance of the instrument. The majority of the laboratories participating in the validation study were able to determine acrylamide in a butter cookie sample at a level of 14,3 µg/kg. Thus, the validation by interlaboratory study showed that LOQ can be expected to be in the range between below 15 µg/kg and 30 µg/kg.




Standard NumberBS EN 16618:2015
TitleFood analysis. Determination of acrylamide in food by liquid chromatography tandem mass spectrometry (LC-ESI-MS/MS)
StatusCurrent
Publication Date30 April 2015
Normative References(Required to achieve compliance to this standard)EN ISO 1042:1999, ISO 1042:1998, EN ISO 3696:1995, ISO 3696:1987
Informative References(Provided for Information)ISO 5725-2:1994
International RelationshipsEN 16618:2015
Draft Superseded By13/30272428 DC
DescriptorsFood products, Liquid chromatography, Mass spectrometry, Agricultural products, Food testing, Chemical analysis and testing, Determination of content
ICS67.050
67.060
67.080.20
67.140.20
Title in FrenchAnalyse des produits alimentaires. Dosage de l'acrylamide dans les produits alimentaires par chromatographie en phase liquide couplée à la spectrométrie de masse en tandem (CL-ESI-SM-SM)
Title in GermanLebensmittelanalytik. Bestimmung von Acrylamid in Lebensmitteln mit Flüssigchromatographie und Tandem- Massenspektrometrie (LC-ESI-MS/MS)
CommitteeAW/275
ISBN978 0 580 80855 5
PublisherBSI
FormatA4
DeliveryYes
Pages28
File Size1.101 MB
Price£182.00


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