BS EN ISO 18857-2:2011 - Water quality. Determination of selected alkylphenols . Gas chromatographic-mass spectrometric determination of alkylphenols, their ethoxylates and bisphenol A in non-filtered samples following solid-phase extraction and derivatisation

BS EN ISO 18857-2:2011

Water quality. Determination of selected alkylphenols . Gas chromatographic-mass spectrometric determination of alkylphenols, their ethoxylates and bisphenol A in non-filtered samples following solid-phase extraction and derivatisation

Status : Current   Published : September 2009

Format
PDF

Format
HARDCOPY



ISO 18857-2:2009 specifies a gas chromatographic-mass spectrometric (GC?MS) determination of selected alkylphenols, their ethoxylates and bisphenol A in non-filtered samples of drinking, ground, surface, and waste waters following solid?phase extraction and derivatisation. The lower limit of the working range depends on the matrix, on the specific compound to be analysed and on the sensitivity of the mass spectrometric detection unit. The method is applicable in a working range from 0,005 µg/l to 0,2 µg/l for 4-(1,1,3,3-tetramethylbutyl)phenol (OP), and its mono- (OP1EO) and diethoxylate (OP2EO), from 0,03 µg/l to 0,2 µg/l for 4-nonylphenol (mixture of isomers) (NP), and its mono- (NP1EO) and diethoxylate (NP2EO), and from 0,05 µg/l to 0,2 µg/l for bisphenol A (BPA). Depending on the matrix, the method is also applicable to waste water in a working range from 0,1 µg/l to 50 µg/l for OP, OP1EO, OP2EO and BPA, and from 0,5 µg/l to 50 µg/l for NP, NP1EO and NP2EO. The working ranges are based on experimental work carried out in ruggedness testing. Water samples containing suspended matter at concentrations of more than 500 mg/l and waste water samples are extracted by passing a 100 ml sample through the cartridge.




Standard NumberBS EN ISO 18857-2:2011
TitleWater quality. Determination of selected alkylphenols . Gas chromatographic-mass spectrometric determination of alkylphenols, their ethoxylates and bisphenol A in non-filtered samples following solid-phase extraction and derivatisation
StatusCurrent
Publication Date30 September 2009
Normative References(Required to achieve compliance to this standard)ISO 3696, ISO 5667-1, ISO 5667-3, ISO 8466-1
Informative References(Provided for Information)ISO 1042
International RelationshipsEN ISO 18857-2:2011,ISO 18857-2:2009
Amended ByCorrigendum, January 2012.
Draft Superseded By08/30154538 DC
DescriptorsWater, Quality, Water testing, Chemical analysis and testing, Determination of content, Phenol, Alkyl compounds, Water resources, Potable water, Ground water, Surface water, Sewage, Gas chromatography, Mass spectrometry, Extraction methods of analysis
ICS13.060.50
Title in FrenchQualité de l'eau. Dosage d'alkylphénols sélectionnés. Dosage par chromatographie en phase gazeuse-spectrométrie de masse d'alkylphénols, de leurs éthoxylates et de bisphénol A dans des échantillons non filtrés après extraction en phase solide et dérivation
Title in GermanWasserbeschaffenheit. Bestimmung von ausgewählten Alkylphenolen. Bestimmung von Alkylphenolen, Alkylphenol-Ethoxylaten und Bisphenol-A. Verfahren für nicht-filtrierte Proben unter Verwendung der Festphasenextraktion und Gaschromatographie mit massenselektiver Detektion nach Derivatisierung
CommitteeEH/3/2
ISBN978 0 580 74618 5
PublisherBSI
FormatA4
DeliveryYes
Pages30
File Size989.4 KB
Price£182.00


 Your basket
Your basket is empty

Multi-user access to over 3,500 medical device standards, regulations, expert commentaries and other documents


Develop a PAS

Develop a fast-track standardization document in 9-12 months


Tracked Changes

Understand the changes made to a standard with our new Tracked Changes version


BSOL

The faster, easier way to work with standards